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GTX5-d: Certified Calibration Solution for Gonyautoxin-5

From National Research Council Canada

Alternative titleGTX5-d : Solution d'étalonnage certifiée pour la gonyautoxine-5
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DOIResolve DOI: https://doi.org/10.4224/crm.2020.gtx5-d.20191024
AuthorSearch for: 1; Search for: 1; Search for: 1; Search for: 1ORCID identifier: https://orcid.org/0000-0002-7746-8432
Affiliation
  1. National Research Council of Canada
Format3D, Material
Material typeCalibration solution
SubjectCanadian reference material; GTX5; Gonyautoxin-5; saxitoxin analogue
Abstract
NRC CRM-GTX5-d is a certified instrument calibration solution for use in the analytical determination of gonyautoxin-5 (GTX5). Each ampoule contains approximately 0.5 mL of a solution of GTX5 dissolved in dilute acetic acid.
Analytes
AnalyteQuantityValueExpanded uncertaintyUnitType
gonyautoxin-5concentration (15-30 °C)53.62.9µmol/Lcertified
Publication date
PublisherNational Research Council of Canada
Copyright statement
  • © 2020 National Research Council of Canada
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References
View items (14)
  1. Hall, Sherwood, Gary Strichartz, E. Moczydlowski, A. Ravindran, and P. B. Reichardt. ‘The Saxitoxins’. Marine Toxins, 29 January 1990, 29–65. .
  2. Shumway, Sandra E. ‘A Review of the Effects of Algal Blooms on Shellfish and Aquaculture’. Journal of the World Aquaculture Society 21, no. 2 (June 1990): 65–104. .
  3. D’Agostino, Paul M., Michael J. Boundy, Tim D. Harwood, Wayne W. Carmichael, Brett A. Neilan, and Susanna A. Wood. ‘Re-Evaluation of Paralytic Shellfish Toxin Profiles in Cyanobacteria Using Hydrophilic Interaction Liquid Chromatography-Tandem Mass Spectrometry’. Toxicon 158 (February 2019): 1–7. .
  4. Laycock, Maurice V., Pierre Thibault, Stephen W. Ayer, and John A. Walter. ‘Isolation and Purification Procedures for the Preparation of Paralytic Shellfish Poisoning Toxin Standards’. Natural Toxins 2, no. 4 (July 1994): 175–83. .
  5. Dell’Aversano, Carmela, Philipp Hess, and Michael A. Quilliam. ‘Hydrophilic Interaction Liquid Chromatography–Mass Spectrometry for the Analysis of Paralytic Shellfish Poisoning (PSP) Toxins’. Journal of Chromatography A 1081, no. 2 (July 2005): 190–201. .
  6. Thomas, Krista M., Daniel G. Beach, Kelley L. Reeves, Ryan S. Gibbs, Elliott S. Kerrin, Pearse McCarron, and Michael A. Quilliam. ‘Hydrophilic Interaction Liquid Chromatography-Tandem Mass Spectrometry for Quantitation of Paralytic Shellfish Toxins: Validation and Application to Reference Materials’. Analytical and Bioanalytical Chemistry 409, no. 24 (20 July 2017): 5675–87. .
  7. Van De Riet, Jeffrey, Ryan S Gibbs, Patricia M Muggah, Wade A Rourke, James D MacNeil, Michael A Quilliam, et al. ‘Liquid Chromatography Post-Column Oxidation (PCOX) Method for the Determination of Paralytic Shellfish Toxins in Mussels, Clams, Oysters, and Scallops: Collaborative Study’. Journal of AOAC INTERNATIONAL 94, no. 4 (1 July 2011): 1154–76. .
  8. Thibault, P., S. Pleasance, and M.V. Laycock. ‘Analysis of Paralytic Shellfish Poisons by Capillary Electrophoresis’. Journal of Chromatography A 542 (January 1991): 483–501. .
  9. Thomas, Krista, Dominik Wechsler, Yi-Min Chen, Sheila Crain, and Michael A Quilliam. ‘Analysis of Natural Toxins by Liquid Chromatography-Chemiluminescence Nitrogen Detection and Application to the Preparation of Certified Reference Materials’. Journal of AOAC INTERNATIONAL 99, no. 5 (1 September 2016): 1173–84. .
  10. Burton, Ian W., Michael A. Quilliam, and John A. Walter. ‘Quantitative 1H NMR with External Standards: Use in Preparation of Calibration Solutions for Algal Toxins and Other Natural Products’. Analytical Chemistry 77, no. 10 (26 March 2005): 3123–31. .
  11. Pauwels, J., A. van der Veen, A. Lamberty, and H. Schimmel. ‘Evaluation of Uncertainty of Reference Materials’. Accreditation and Quality Assurance 5, no. 3 (3 March 2000): 95–99. .
  12. Pauwels, Jean, Andrée Lamberty, and Heinz Schimmel. ‘The Determination of the Uncertainty of Reference Materials Certified by Laboratory Intercomparison’. Accreditation and Quality Assurance 3, no. 5 (4 May 1998): 180–84. .
  13. Ellison, S. L. R., S. Burke, R. F. Walker, K. Heydorn, M. Månsson, J. Pauwels, W. Wegscheider, and B. te Nijenhuis. ‘Uncertainty for Reference Materials Certified by Interlaboratory Study: Recommendations of an International Study Group’. Accreditation and Quality Assurance 6, no. 6 (18 May 2001): 274–77. .
  14. Evaluation of measurement data – Supplement 1 to the “Guide to the expression of uncertainty in measurement” (GUM) – Propagation of distributions using a Monte Carlo method (1 January 2008). .
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CollectionCanadian Reference Materials and Methods
Record identifierfbf7c1de-bebe-42b9-8543-cc9c53dac1af
Record created2020-12-02
Record modified2025-04-22
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