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GTX2&3-d: Certified Calibration Solution for Gonyautoxins-2 and -3

From National Research Council Canada

Alternative titleGTX2&3-d : Solution d’étalonnage certifiée pour les gonyautoxines-2 et -3
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DOIResolve DOI: https://doi.org/10.4224/crm.2017.gtx2-3-d.20170419
AuthorSearch for: 1; Search for: 1; Search for: 1; Search for: 1; Search for: 1ORCID identifier: https://orcid.org/0000-0002-7746-8432
Affiliation
  1. National Research Council Canada
Format3D, Material
Material typeCalibration solution
SubjectCanadian reference material; gonyautoxin-2; gonyautoxin-3
Abstract
CRM-GTX2&3-d is a certified instrument calibration solution prepared to aid the analyst in the determination of GTX2 and GTX3. Each ampoule contains a solution of GTX2 and GTX3 dissolved in filtered, aqueous 0.5 mM hydrochloric acid (HCl).
Analytes
AnalyteQuantityValueExpanded uncertaintyUnitType
gonyautoxin-2concentration (25 °C)102.64.0µmol/Lcertified
gonyautoxin-3concentration (25 °C)43.52.9µmol/Lcertified
gonyautoxin-2 and gonyautoxin-3concentration (25 °C)146.16.9µmol/Lcertified
gonyautoxin-1concentration (25 °C)0.21µmol/Linformation
gonyautoxin-4concentration (25 °C)0.03µmol/Linformation
decarbamoylgonyautoxin-2concentration (25 °C)0.23µmol/Linformation
decarbamoylgonyautoxin-3concentration (25 °C)0.13µmol/Linformation
Publication date
PublisherNational Research Council Canada
Copyright statement
  • © 2017 National Research Council Canada
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References
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  3. Van De Riet, Jeffrey, Ryan S Gibbs, Patricia M Muggah, Wade A Rourke, James D MacNeil, Michael A Quilliam, et al. ‘Liquid Chromatography Post-Column Oxidation (PCOX) Method for the Determination of Paralytic Shellfish Toxins in Mussels, Clams, Oysters, and Scallops: Collaborative Study’. Journal of AOAC INTERNATIONAL 94, no. 4 (1 July 2011): 1154–76. .
  4. Thomas, Krista M., Daniel G. Beach, Kelley L. Reeves, Ryan S. Gibbs, Elliott S. Kerrin, Pearse McCarron, and Michael A. Quilliam. ‘Hydrophilic Interaction Liquid Chromatography-Tandem Mass Spectrometry for Quantitation of Paralytic Shellfish Toxins: Validation and Application to Reference Materials’. Analytical and Bioanalytical Chemistry 409, no. 24 (20 July 2017): 5675–87. .
  5. Thibault, P., S. Pleasance, and M.V. Laycock. ‘Analysis of Paralytic Shellfish Poisons by Capillary Electrophoresis’. Journal of Chromatography A 542 (January 1991): 483–501. .
  6. Thomas, Krista, Dominik Wechsler, Yi-Min Chen, Sheila Crain, and Michael A Quilliam. ‘Analysis of Natural Toxins by Liquid Chromatography-Chemiluminescence Nitrogen Detection and Application to the Preparation of Certified Reference Materials’. Journal of AOAC INTERNATIONAL 99, no. 5 (1 September 2016): 1173–84. .
  7. Burton, Ian W., Michael A. Quilliam, and John A. Walter. ‘Quantitative 1H NMR with External Standards: Use in Preparation of Calibration Solutions for Algal Toxins and Other Natural Products’. Analytical Chemistry 77, no. 10 (26 March 2005): 3123–31. .
  8. Pauwels, J., A. van der Veen, A. Lamberty, and H. Schimmel. ‘Evaluation of Uncertainty of Reference Materials’. Accreditation and Quality Assurance 5, no. 3 (3 March 2000): 95–99. .
  9. Pauwels, Jean, Andrée Lamberty, and Heinz Schimmel. ‘The Determination of the Uncertainty of Reference Materials Certified by Laboratory Intercomparison’. Accreditation and Quality Assurance 3, no. 5 (4 May 1998): 180–84. .
  10. Ellison, S. L. R., S. Burke, R. F. Walker, K. Heydorn, M. Månsson, J. Pauwels, W. Wegscheider, and B. te Nijenhuis. ‘Uncertainty for Reference Materials Certified by Interlaboratory Study: Recommendations of an International Study Group’. Accreditation and Quality Assurance 6, no. 6 (18 May 2001): 274–77. .
  11. Evaluation of measurement data – Guide to the expression of uncertainty in measurement (GUM), JCGM 100:2008 (corrected version 2010) (1 September 2008). .
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CollectionCanadian Reference Materials and Methods
Record identifiere0d35a2e-62aa-4298-a0c8-9896e87a40c4
Record created2022-02-24
Record modified2025-11-20
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