| Alternative title | BBET-1 : Matériau de référence certifié - bromure d'arsénobétaine marqué au carbone-13 |
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| DOI | Resolve DOI: https://doi.org/10.4224/crm.2016.bbet-1 |
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| Author | Search for: Le, Phuong Mai1ORCID identifier: https://orcid.org/0000-0002-6101-5252; Search for: Leek, Donald1; Search for: Mester, Zoltan1ORCID identifier: https://orcid.org/0000-0002-2377-2615; Search for: Windust, Anthony1; Search for: Meija, Juris1ORCID identifier: https://orcid.org/0000-0002-3349-5535 |
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| Affiliation | - National Research Council Canada
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| Format | 3D, Material |
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| Material type | High-purity material |
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| Subject | Canadian reference material; BBET-1; arsenobetaine; carbon-13 |
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| Abstract | BBET-1 is a high-purity certified reference material (CRM) of carbon-13 labelled arsenobetaine bromide from the National Research Council of Canada (NRC), intended for analytical method development and accurate quantitation of arsenobetaine. A unit of this material consists of approximately 30 mg. Certified and information values are based on results from data generated at NRC using quantitative proton nuclear magnetic resonance spectroscopy (1H-qNMR) and chemical specifications. |
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| Analytes | | Analyte | Quantity | Value | Expanded uncertainty | Unit | Type |
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| [13CH2]-arsenobetaine bromide | mass fraction | 0.9902 | 0.0086 | g/g | certified | | [13CH2]-arsenobetaine (cation) | mass fraction | 0.6858 | 0.0060 | g/g | certified | | ethanol | mass fraction | 0.0006 | | g/g | information |
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| Period of validity | - Valid from 2026-02-23 until 2036-03-31
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| Publication date | 2016-02-01 |
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| Publisher | National Research Council Canada |
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| Copyright statement | - © 2016 National Research Council Canada
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| References | View items (4)- Minhas, R., D. S. Forsyth, and B. Dawson. ‘Synthesis and Characterization of Arsenobetaine and Arsenocholine Derivatives’. Applied Organometallic Chemistry 12, no. 8–9 (August 1998): 635–41. https://doi.org/10.1002/(sici)1099-0739(199808/09)12:8/9<635::aid-aoc772>3.0.co;2-j.
- Le, Phuong-Mai, Jianfu Ding, Donald M. Leek, Zoltan Mester, Gilles Robertson, Anthony Windust, and Juris Meija. ‘Determination of Chemical Purity and Isotopic Composition of Natural and Carbon-13-Labeled Arsenobetaine Bromide Standards by Quantitative1H-NMR’. Analytical and Bioanalytical Chemistry 408, no. 26 (11 August 2016): 7413–21. https://doi.org/10.1007/s00216-016-9827-y.
- ‘Evaluation of Measurement Data — Guide to the Expression of Uncertainty in Measurement’, 2008. https://doi.org/10.59161/jcgm100-2008e.
- DerSimonian, Rebecca, and Nan Laird. ‘Meta-Analysis in Clinical Trials’. Controlled Clinical Trials 7, no. 3 (September 1986): 177–88. https://doi.org/10.1016/0197-2456(86)90046-2.
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| Referenced by | View items (1)- Kumkrong, Paramee, Benjaporn Thiensong, Phuong Mai Le, Garnet McRae, Anthony Windust, Suladda Deawtong, Juris Meija, Paulette Maxwell, Lu Yang, and Zoltán Mester. ‘Species Specific Isotope Dilution for the Accurate and SI Traceable Determination of Arsenobetaine and Methylmercury in Cuttlefish and Prawn’. Analytica Chimica Acta 943 (November 2016): 41–49. https://doi.org/10.1016/j.aca.2016.09.031.
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| Export citation | Export as RIS |
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| Collection | Canadian Reference Materials and Methods |
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| Record identifier | 949f9057-b516-47b3-b6fa-19ce7aeba926 |
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| Record created | 2018-05-31 |
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| Record modified | 2026-02-23 |
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