| Alternative title | OA-d : Solution d’étalonnage certifiée pour l’acide okadaïque |
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| DOI | Resolve DOI: https://doi.org/10.4224/crm.2015.oa-d.20141119 |
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| Author | Search for: Crain, Sheila1ORCID identifier: https://orcid.org/0000-0002-2175-6929; Search for: Perez, Ruth1; Search for: LeBlanc, Patricia1; Search for: Quilliam, Michael1; Search for: Beach, Daniel G1ORCID identifier: https://orcid.org/0000-0002-5680-2112; Search for: McCarron, Pearse1ORCID identifier: https://orcid.org/0000-0002-7746-8432 |
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| Affiliation | - National Research Council of Canada
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| Format | 3D, Material |
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| Material type | Calibration solution |
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| Subject | Canadian reference material; okadaic acid; CRM-OA-d |
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| Abstract | CRM-OA-d is a certified calibration solution designed for analytical method development and accurate quantitation of OA. The concentration of CRM-OA-d makes it suitable for preparing a dilution series for calibration of liquid chromatography (LC) and liquid chromatography-mass spectrometry (LC-MS) instrumentation, as well as for spiking shellfish control samples for recovery experiments. |
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| Analytes | | Analyte | Quantity | Value | Expanded uncertainty | Unit | Type |
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| okadaic acid | mass fraction | 10.6 | 0.5 | µg/g | certified | | okadaic acid | mass concentration (20 °C) | 8.4 | 0.4 | µg/mL | certified | | okadaic acid | concentration (20 °C) | 10.4 | 0.5 | µmol/L | certified |
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| Publication date | 2015-07-27 |
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| Publisher | National Research Council of Canada |
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| Copyright statement | - © 2015
National Research Council of Canada
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| Access condition | |
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| References | View items (7)- Regulation (EC) No 853/2004 of the European parliament and of the council of 29 April 2004 laying down specific hygiene rules for food of animal origin (30 April 2004). https://eur-lex.europa.eu/LexUriServ/LexUriServ.do?uri=OJ:L:2004:139:0055:0205:en:PDF.
- Murata, Michio, Miho Izumikawa, Kazuo Tachibana, Tsuyoshi Fujita, and Hideo Naoki. ‘Labeling Pattern of Okadaic Acid from 18O2 and [18O2]Acetate Elucidated by Collision-Induced Dissociation Tandem Mass Spectrometry’. Journal of the American Chemical Society 120, no. 1 (1 January 1998): 147–51. https://doi.org/10.1021/ja971547p.
- Burton, Ian W., Michael A. Quilliam, and John A. Walter. ‘Quantitative 1H NMR with External Standards: Use in Preparation of Calibration Solutions for Algal Toxins and Other Natural Products’. Analytical Chemistry 77, no. 10 (26 March 2005): 3123–31. https://doi.org/10.1021/ac048385h.
- ISO Guide 35 (2006). Reference materials - general and statistical principles for certification (1 January 2006). https://www.iso.org/standard/39269.html.
- Pauwels, Jean, Andrée Lamberty, and Heinz Schimmel. ‘The Determination of the Uncertainty of Reference Materials Certified by Laboratory Intercomparison’. Accreditation and Quality Assurance 3, no. 5 (4 May 1998): 180–84. https://doi.org/10.1007/s007690050218.
- Pauwels, J., A. van der Veen, A. Lamberty, and H. Schimmel. ‘Evaluation of Uncertainty of Reference Materials’. Accreditation and Quality Assurance 5, no. 3 (3 March 2000): 95–99. https://doi.org/10.1007/s007690050020.
- ‘Marine biotoxins in shellfish - okadaic acid and analogues - Scientific Opinion of the Panel on Contaminants in the Food chain’. JD. EFSA Journal, no. EFSA Journal (n.d.). https://doi.org/10.2903/j.efsa.2008.589.
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| Export citation | Export as RIS |
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| Collection | Canadian Reference Materials and Methods |
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| Record identifier | 33eeba13-2343-44be-a073-d0ede056b1d9 |
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| Record created | 2022-04-05 |
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| Record modified | 2025-05-14 |
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