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AZA3-b: Certified Calibration Solution for Azaspiracid-3

From National Research Council Canada

Alternative titleAZA3-b : Solution d’étalonnage certifiée pour l’azaspiracide-3
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DOIResolve DOI: https://doi.org/10.4224/crm.2016.aza3-b.20150527
AuthorSearch for: 1; Search for: 1ORCID identifier: https://orcid.org/0000-0002-2175-6929; Search for: 1; Search for: 1; Search for: 1ORCID identifier: https://orcid.org/0000-0002-7746-8432
Affiliation
  1. National Research Council of Canada
Format3D, Material
Material typeCalibration solution
SubjectCanadian reference material; azaspiracid-3; azaspiracids
Abstract
CRM-AZA3-b is designed for use as an instrument calibration solution to aid the analyst in the determination of AZA3 in plankton and shellfish sample extracts. The most widely used method of analysis is liquid chromatography-mass spectrometry (LC-MS) and the concentration of AZA3 in CRM AZA3-b is suitable for the calibration of most LC-MS instruments. CRM-AZA3-b can also be used for spiking shellfish control samples for recovery experiments.
Analytes
AnalyteQuantityValueExpanded uncertaintyUnitType
azaspiracid-3 and 37-epi-azaspiracid-3mass fraction1.510.06µg/gcertified
azaspiracid-3 and 37-epi-azaspiracid-3mass concentration (20 °C)1.180.05µg/mLcertified
azaspiracid-3 and 37-epi-azaspiracid-3concentration (20 °C)1.430.06µmol/Lcertified
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PublisherNational Research Council of Canada
Copyright statement
  • © 2016 National Research Council of Canada
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References
View items (9)
  1. Winter toxicity of unknown aetiology in mussels (1 January 1996). .
  2. AZASPIRACIDS - Toxicological Evaluation, Test Methods and Identification of the Source Organisms (ASTOX II) (1 January 2014). .
  3. Satake, Masayuki, Katsuya Ofuji, Hideo Naoki, Kevin J. James, Ambrose Furey, Terry McMahon, Joe Silke, and Takeshi Yasumoto. ‘Azaspiracid, a New Marine Toxin Having Unique Spiro Ring Assemblies, Isolated from Irish Mussels, Mytilus Edulis’. Journal of the American Chemical Society 120, no. 38 (1 September 1998): 9967–68. .
  4. Nicolaou, K. C., Theocharis V. Koftis, Stepan Vyskocil, Goran Petrovic, Wenjun Tang, Michael O. Frederick, David Y.-K. Chen, Yiwei Li, Taotao Ling, and Yoichi M. A. Yamada. ‘Total Synthesis and Structural Elucidation of Azaspiracid-1. Final Assignment and Total Synthesis of the Correct Structure of Azaspiracid-1’. Journal of the American Chemical Society 128, no. 9 (2 February 2006): 2859–72. .
  5. Tillmann, Urban, Malte Elbrächter, Bernd Krock, Uwe John, and Allan Cembella. ‘Azadinium SpinosumGen. et Sp. Nov. (Dinophyceae) Identified as a Primary Producer of Azaspiracid Toxins’. European Journal of Phycology 44, no. 1 (February 2009): 63–79. .
  6. Regulation (EC) No 853/2004 of the European parliament and of the council of 29 April 2004 laying down specific hygiene rules for food of animal origin (30 April 2004). .
  7. Burton, Ian W., Michael A. Quilliam, and John A. Walter. ‘Quantitative 1H NMR with External Standards: Use in Preparation of Calibration Solutions for Algal Toxins and Other Natural Products’. Analytical Chemistry 77, no. 10 (26 March 2005): 3123–31. .
  8. Kilcoyne, Jane, Pearse McCarron, Michael J. Twiner, Ciara Nulty, Sheila Crain, Michael A. Quilliam, Frode Rise, Alistair L. Wilkins, and Christopher O. Miles. ‘Epimers of Azaspiracids: Isolation, Structural Elucidation, Relative LC-MS Response, and in Vitro Toxicity of 37-Epi-Azaspiracid-1’. Chemical Research in Toxicology 27, no. 4 (7 February 2014): 587–600. .
  9. Pauwels, J., A. van der Veen, A. Lamberty, and H. Schimmel. ‘Evaluation of Uncertainty of Reference Materials’. Accreditation and Quality Assurance 5, no. 3 (3 March 2000): 95–99. .
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CollectionCanadian Reference Materials and Methods
Record identifier2941729f-4396-41e0-a4fa-443b1ac4157b
Record created2022-03-15
Record modified2025-04-17
Date modified: