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AZA2-b: Certified Calibration Solution for Azaspiracid-2

From National Research Council Canada

Alternative titleAZA2-b : Solution d’étalonnage certifiée pour l’azaspiracide-2
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DOIResolve DOI: https://doi.org/10.4224/crm.2015.aza2-b.20131126
AuthorSearch for: 1ORCID identifier: https://orcid.org/0000-0002-2175-6929; Search for: 1; Search for: 1; Search for: 1; Search for: 1ORCID identifier: https://orcid.org/0000-0002-7746-8432
Affiliation
  1. National Research Council of Canada
Format3D, Material
Material typeCalibration solution
SubjectCanadian reference material; azaspiracid-2; azaspiracids
Abstract
CRM-AZA2-b is designed for use as an instrument calibration solution to aid the analyst in the determination of AZA2 in plankton and shellfish sample extracts. The most widely used method of analysis is liquid chromatography-mass spectrometry (LC-MS) and the concentration of AZA2 in CRM AZA2-b is suitable for the calibration of most LC-MS instruments. CRM-AZA2-b can also be used for spiking shellfish control samples for recovery experiments.
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PublisherNational Research Council of Canada
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  • © 2015 National Research Council of Canada
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References
View items (9)
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  5. Tillmann, Urban, Malte Elbrächter, Bernd Krock, Uwe John, and Allan Cembella. ‘Azadinium SpinosumGen. et Sp. Nov. (Dinophyceae) Identified as a Primary Producer of Azaspiracid Toxins’. European Journal of Phycology 44, no. 1 (February 2009): 63–79. .
  6. Regulation (EC) No 853/2004 of the European parliament and of the council of 29 April 2004 laying down specific hygiene rules for food of animal origin (30 April 2004). .
  7. Burton, Ian W., Michael A. Quilliam, and John A. Walter. ‘Quantitative 1H NMR with External Standards: Use in Preparation of Calibration Solutions for Algal Toxins and Other Natural Products’. Analytical Chemistry 77, no. 10 (26 March 2005): 3123–31. .
  8. Kilcoyne, Jane, Pearse McCarron, Michael J. Twiner, Ciara Nulty, Sheila Crain, Michael A. Quilliam, Frode Rise, Alistair L. Wilkins, and Christopher O. Miles. ‘Epimers of Azaspiracids: Isolation, Structural Elucidation, Relative LC-MS Response, and in Vitro Toxicity of 37-Epi-Azaspiracid-1’. Chemical Research in Toxicology 27, no. 4 (7 February 2014): 587–600. .
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CollectionCanadian Reference Materials and Methods
Record identifier1e69df41-bf3a-4495-abf8-9b3a23fb6c52
Record created2022-03-15
Record modified2025-04-16
Date modified: